Hydrazine hydrate (1:1) → HCID 21249171、化合物

HRID 1194674ノート

反応式

HRID 1194674 の反応式
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=O)[CH:10]([CH3:15])[CH2:11][C:12](O)=[O:13])=[CH:5][CH:4]=1.O.[NH2:18][NH2:19]>C(O)(C)C>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:10]([CH3:15])[CH2:11][C:12](=[O:13])[NH:18][N:19]=2)=[CH:5][CH:4]=1

参加物

4

反応物 2

HCID 24654Hydrazine hydrate (1:1)HCID 13693406HCID 13693406、化合物

生成物 1

HCID 21249171HCID 21249171、化合物

試薬・触媒・溶媒 1

HCID 3776Isopropanol溶媒

実験手順

2.3 g (0.01 mole) of 4-(4-methylthio-phenyl)-4-oxo-3-methyl-butyric acid and 1 ml of hydrazine hydrate are heated under reflux in 20 ml of isopropanol for 2 hour. After the mixture has been cooled, the product is filtered off with suction and dried.

後処理

  1. temperatureAfter the mixture has been cooled
  2. filtrationthe product is filtered off with suction
  3. customdried

出典と根拠

ORDレコード
ord-fdb03b77d58940cf8d186e5619f473b4
出典データセット
uspto-grants-1989_03
特許番号
US04816454

反応ノート

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