Benzoyl Peroxide → HCID 14368704、化合物
反応式
[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH3:13].[Br:14]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH2:13][Br:14]参加物
5
実験手順
1.35 g of 5,7-Difluoro-1-methylnaphthaline in 10 ml of carbon tetrachloride are refluxed for 41/2 hours with 1.4 g of N-bromosuccinimide and 50 mg of dibenzoylperoxide. The cooled mixture is filtered and the solvent removed under vacuum. The purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°.
後処理
- filtrationThe cooled mixture is filtered
- customthe solvent removed under vacuum
- customThe purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°
出典と根拠
- ORDレコード
- ord-8c79336066a24a918e8010e041886d60
- 出典データセット
- uspto-grants-1992_05
- 特許番号
- US05112851
反応ノート
読み込み中…