化工社化工社 化学情報印刷レポート · 研究参考用
1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone → 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone | HCID 301557 | — |
| 反応物 | Sodium hypobromite | HCID 23673712 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid | HCID 2759552 | 90% |
反応手順
A solution of 18 g of 4-acetyl-4'-methoxybiphenyl in 285 ml of dioxane was oxidized with a dilute sodium hypobromite. Recrystallization from ethanol and acetic acid gave 4'-methoxybiphenyl-4-carboxylic acid melting at 285° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05114613 |
| 出典データセット | uspto-grants-1992_05 |
| ORD ID | ord-815353fc731c4aa0a12ab6f1fe7a78a7 |
| 出典メモ | uspto-grants-1992_05 |