HRID1196438

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID301557

1-(4'-Methoxy[1,1'-biphenyl]-4-yl)ethan-1-one

C15H14O2

HCID23673712

Sodium hypobromite

BrNaO

PRODUCTS

生成物

HCID2759552

4'-Methoxy[1,1'-biphenyl]-4-carboxylic acid

C14H12O3

收率 90%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A solution of 18 g of 4-acetyl-4'-methoxybiphenyl in 285 ml of dioxane was oxidized with a dilute sodium hypobromite. Recrystallization from ethanol and acetic acid gave 4'-methoxybiphenyl-4-carboxylic acid melting at 285° C.

WORKUP

后处理

customRecrystallization from ethanol and acetic acid