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Dicyclohexylcarbodiimide → 4-(1-Methylheptyloxycarbonyl)phenyl 4'-n-Nonanoyloxybiphenyl-4-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 反応物 | 4-(1-Methylheptyloxycarbonyl)phenol | HCID 11010379 | — |
| 反応物 | 4'-Nonanoyloxybiphenyl-4-carboxylic acid | HCID 13668451 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 4-(1-Methylheptyloxycarbonyl)phenyl 4'-n-Nonanoyloxybiphenyl-4-carboxylate | HCID 15919277 | — |
反応手順
In 330 ml of dehydrated tetrahydrofuran were dissolved 5.00 g of 4'-nonanoyloxybiphenyl-4-carboxylic acid and 6.76 g of 1-methylheptyl 4-hydroxybenzoate synthesized in (2) above. To the solution were added 6.18 g of DCC and 0.24 g of dimethylaminopyridine, followed by stirring for one day at room temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05116531 |
| 出典データセット | uspto-grants-1992_05 |
| ORD ID | ord-bf99518655ed4455b7ae0f2d46f54000 |
| 出典メモ | uspto-grants-1992_05 |