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Potassium Carbonate → HCID 178418677、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-Butoxy-2,3-difluorophenol | HCID 19103433 | — |
| 反応物 | HCID 178444389 | HCID 178444389 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 178418677 | HCID 178418677 | — |
反応手順
0.1 mol of 2,3-difluoro-4-butoxyphenol, 0.11 mol of trans-4-pentylcyclohexylmethyl bromide and 0.11 mol of potassium carbonate are heated at 100° in 100 ml of dimethylformamide (DMF) for 16 hours. After cooling, the inorganic salts are filtered off with suction, the filtrate is concentrated and water is added. Extraction with methylene chloride gives 1-butoxy-2,3-difluoro-4-(trans-4-pentylcyclohexylmethoxy)benzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05279764 |
| 出典データセット | uspto-grants-1994_01 |
| ORD ID | ord-1bae8b3220744c4abf0f5bfe7aab8377 |
| 出典メモ | uspto-grants-1994_01 |