4-(3-Methoxyphenyl)but-3-en-2-one → 4-(3-Methoxyphenyl)butan-2-one
反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11](=[O:13])[CH3:12])[CH:6]=[CH:7][CH:8]=1>CO.[Pd]>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][C:11](=[O:13])[CH3:12])[CH:6]=[CH:7][CH:8]=1参加物
4
実験手順
A solution of 30.1 g of 4-(3-methoxyphenyl)-3-buten-2-one in 200 ml of MeOH was hydrogenated over 200 mg of 10% palladium on carbon for two hours. The catalyst was filtered and the solvent evaporated in vacuo to give 30.2 g of yellow oily 4-(3-methoxyphenyl)-2-butanone.
後処理
- filtrationThe catalyst was filtered
- customthe solvent evaporated in vacuo
出典と根拠
- ORDレコード
- ord-61ca01d144964a2e98ce71468bfe29b1
- 出典データセット
- uspto-grants-1990_02
- 特許番号
- US04898889
反応ノート
読み込み中…