2-Naphthoyl chloride → HCID 10083909、化合物
反応式
[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH2:5].[CH:7]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:10]=[CH:9][C:8]=1[C:17](Cl)=[O:18]>N1C=CC=CC=1>[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH:5][C:17]([C:8]1[CH:9]=[CH:10][C:11]2[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:7]=1)=[O:18]参加物
4
実験手順
To a stirred room temperature solution of 4-methylthiosemicarbazide (5.91 g, 5.62×10-2 mole) and pyridine (150 ml) was added 2-naphthoyl chloride (10.7 g, 5.61×10-2 mole). After stirring overnight, the pyridine was evaporated at reduced pressure. The concentrate was treated with water and the undissolved product was collected by filtration and dried by suction.
後処理
- customthe pyridine was evaporated at reduced pressure
- additionThe concentrate was treated with water
- filtrationthe undissolved product was collected by filtration
- customdried by suction
出典と根拠
- ORDレコード
- ord-c9281fd746634014bc2368dea7eb7761
- 出典データセット
- uspto-grants-1990_02
- 特許番号
- US04900743
反応ノート
読み込み中…