Carbon Disulfide → HCID 178507537、化合物

HRID 1241905

反応式

HRID 1241905 の反応式
[NH2:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][CH:11]=1)[C:5]([NH:7][NH2:8])=[O:6].C(N(CC)CC)C.[C:19](=S)=[S:20]>C(O)C>[NH2:1][C:2]1[CH:3]=[C:4]([C:5]2[O:6][C:19]([SH:20])=[N:8][N:7]=2)[CH:9]=[CH:10][CH:11]=1

参加物

5

反応物 3

HCID 6348Carbon DisulfideHCID 8471TriethylamineHCID 84178m-Aminobenzohydrazide

生成物 1

HCID 178507537HCID 178507537、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

3-Aminobenzhydrazide (5.76 g) was dissolved in ethanol (40 mL), and triethylamine (4.8 mL) and carbon disulfide (2.1 mL) were added to the solution. The mixture was heated under reflux for 4 hrs. The solvent was evaporated, and water was added. The precipitated solids were collected by filtration to give the title compound (5.06 g) as a pale-yellow powder.

後処理

  1. temperatureThe mixture was heated
  2. temperatureunder reflux for 4 hrs
  3. customThe solvent was evaporated
  4. additionwater was added
  5. filtrationThe precipitated solids were collected by filtration

出典と根拠

ORDレコード
ord-2272d54bcda141169e47c2ffb68a7bea
出典データセット
uspto-grants-2006_10
特許番号
US07115635B2

関連ノート

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