1,5-Pentanediol → 3,5-Dimethyl-1-hexyn-3-ol

HRID 1245234

反応式

HRID 1245234 の反応式
[CH2:1](O)CCCCO.C(O)C(O)CCCC.N1CCCC1=O.CCCCC([CH2:29][CH2:30][CH:31]([O:36]S([O-])(=O)=O)[CH2:32][CH:33]([CH3:35])[CH3:34])CC.[Na+]>O>[CH3:35][CH:33]([CH2:32][C:31]([OH:36])([C:30]#[CH:29])[CH3:1])[CH3:34]

参加物

6

反応物 4

HCID 81051,5-PentanediolHCID 120252-PyrrolidoneHCID 943351,2-HexanediolHCID 23665772Sodium Tetradecyl Sulfate

生成物 1

HCID 610183,5-Dimethyl-1-hexyn-3-ol収率 188.1%

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Ink I-1 containing inventive Dye 1 was prepared by dissolving 0.57 g dye, 1 g 1,5-pentanediol, 0.2 g 1,2-hexanediol, 0.6 g 2-pyrrolidinone, 0.04 g Tergitol 15-S-9 and 0.03 g Surfynol 465® (Air Products Co.) in enough water to give a total weight of 10 g. Ink I-2 was made in the same way except 0.52 g of inventive Dye 2 was used.

後処理

  1. additionInk I-1 containing inventive Dye 1
  2. customwas prepared
  3. dissolutionby dissolving 0.57 g

出典と根拠

ORDレコード
ord-cd576fe8ea014f94b5c0546f3e6920e5
出典データセット
uspto-grants-2006_10
特許番号
US07125446B2

関連ノート

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