Ethanolamine → N-(3,7,11,15-Tetramethyl-6,10,14-hexadecatrienoyl)-ethanolamine

反応式

[CH3:1][CH:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])[CH2:3][C:4]([OH:6])=O.[CH2:23]([CH2:25][NH2:26])[OH:24]>>[CH3:1][CH:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])[CH2:3][C:4]([NH:26][CH2:25][CH2:23][OH:24])=[O:6]

参加物

反応物 2

HCID 700Ethanolamine

HCID 54445755HCID 54445755、化合物

生成物 1

HCID 54091898N-(3,7,11,15-Tetramethyl-6,10,14-hexadecatrienoyl)-ethanolamine収率 92%

実験手順

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-6,10,14-hexadecatrienoic acid and 1.8 ml of ethanolamine were used as starting materials. 6.4 g (yield 92%) of the title compound was obtained as a colorless oil.

出典と根拠

ORDレコード: ord-3dddce49dedd41699cfe599174935eee
出典データセット: uspto-grants-1988_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04742058

反応ノート

読み込み中…