Methylhydrazine → Ethyl 2-(1-methylhydrazinyl)acetate

HRID 1254477ノート

反応式

HRID 1254477 の反応式
[CH3:1][NH:2][NH2:3].Br[CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7]>>[CH3:1][N:2]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])[NH2:3]

参加物

3

反応物 2

HCID 6061MethylhydrazineHCID 7748Ethyl bromoacetate

生成物 1

HCID 20288078Ethyl 2-(1-methylhydrazinyl)acetate収率 77.2%

実験手順

According to the procedure described in the synthesis method of Compound XV-1 with the modification that the reaction was carried out overnight, methylhydrazine 7.13 ml (150 mmol) was reacted with ethyl 2-bromoacetate 16.7 g (100 mmol) to obtain the title compound 10.2 g (77%).

後処理

  1. customdescribed in the synthesis method of Compound XV-1 with the modification that the reaction

出典と根拠

ORDレコード
ord-186cc4c135604f159249530031554b32
出典データセット
uspto-grants-2013_06
特許番号
US08455488B2

反応ノート

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