Nitric Acid → 1,1,3,5,5,7-Hexanitro-3,7-diazacyclooctane
反応式
[N+:1]([C:4]1([N+:20]([O-:22])=[O:21])[CH2:11][NH:10][CH2:9][C:8]([N+:15]([O-:17])=[O:16])([N+:12]([O-:14])=[O:13])[CH2:7][N:6]([N:18]=[O:19])[CH2:5]1)([O-:3])=[O:2].S(=O)(=O)(O)[OH:24].[N+:28]([O-])([OH:30])=[O:29]>>[N+:18]([N:6]1[CH2:7][C:8]([N+:15]([O-:17])=[O:16])([N+:12]([O-:14])=[O:13])[CH2:9][N:10]([N+:28]([O-:30])=[O:29])[CH2:11][C:4]([N+:1]([O-:3])=[O:2])([N+:20]([O-:22])=[O:21])[CH2:5]1)([O-:24])=[O:19]参加物
4
実験手順
nitrating the 3,3,7,7-tetranitro-1-nitrosoperhydro-1,5-diazocine in a mixture of concentrated sulfuric acid and 90% nitric acid at a temperature of from about 0° C. to about 5° C. to form 1,3,3,5,7,7-hexanitroperhydro-1,5-diazocine; and
出典と根拠
- ORDレコード
- ord-9043644e562241f6b64386cc9cc03c3d
- 出典データセット
- uspto-grants-1984_06