Hydrazine hydrate (1:1) → 2-(3,5-Dimethylmorpholino)ethylamine

反応式

[CH3:1][CH:2]1[N:7]([CH2:8][CH2:9][N:10]2C(=O)C3C(=CC=CC=3)C2=O)[CH:6]([CH3:21])[CH2:5][O:4][CH2:3]1.O.NN>>[CH3:21][CH:6]1[N:7]([CH2:8][CH2:9][NH2:10])[CH:2]([CH3:1])[CH2:3][O:4][CH2:5]1

参加物

反応物 2

HCID 24654Hydrazine hydrate (1:1)

HCID 234412322-[2-(3,5-dimethylmorpholino)ethyl]-1H-isoindole-1,3(2H)-dione

生成物 1

HCID 120961382-(3,5-Dimethylmorpholino)ethylamine

実験手順

The title compound was prepared by a similar method to Preparation 7 from 2-[2-(3,5-dimethylmorpholino)ethyl]-1H-isoindole-1,3(2H)-dione [see Preparation 11] and hydrazine hydrate, to afford 2-(3,5-dimethylmorpholino)ethylamine as a white solid.

出典と根拠

ORDレコード: ord-6e320c7aded340219a16331ef0daed60
出典データセット: uspto-grants-2000_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06166011

反応ノート

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