Sodium Hydroxide → Sodium 4-(allylamino)phenylacetate
反応式
[CH2:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([CH2:11][C:12]([OH:14])=[O:13])=[CH:7][CH:6]=1)[CH:2]=[CH2:3].[OH-].[Na+:16]>O.C(O)C>[CH2:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([CH2:11][C:12]([O-:14])=[O:13])=[CH:7][CH:6]=1)[CH:2]=[CH2:3].[Na+:16]参加物
4
実験手順
A mixture of 3.62 g. of 4-(allylamino)phenylacetic acid and 25 ml. of ethanol water (9:1) containing 0.400 g. of sodium hydroxide is stirred for 4 hours. The mixture is filtered and the residue washed with 10 ml. of ethanol-water (9:1) and dried in vacuo for 24 hours to yield sodium 4-(allylamino)phenylacetate as a white solid.
後処理
- additionA mixture of 3.62 g
- filtrationThe mixture is filtered
- washthe residue washed with 10 ml
- dry with materialof ethanol-water (9:1) and dried in vacuo for 24 hours
出典と根拠
- ORDレコード
- ord-9f6926eaab14403a8e5c014dd4ff83e9
- 出典データセット
- uspto-grants-1981_07
- 特許番号
- US04281019
反応ノート
読み込み中…