化工社化工社 化学情報印刷レポート · 研究参考用
Methacrylic Acid → 2-Methylidene-5-phenylpent-4-enoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methacrylic Acid | HCID 4093 | — |
| 反応物 | Styrene | HCID 7501 | — |
| 生成物 | 2-Methylidene-5-phenylpent-4-enoic acid | HCID 53969979 | — |
反応手順
After reaction at a temperature of 75° C. for one hour, a mixture of 1232 g of styrene and 28 g of methacrylic acid was continuously charged thereinto over a period of 4 hours and the reaction was continued at 75° C. for 3 hours, after which the reaction mixture was cooled to room temperature to obtain an aqueous dispersion of styrene-methacrylic acid copolymer particles. The solid concentration of the aqueous dispersion was 20%. The mean particle size of the polymer particles was 0.19 μm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06454819B1 |
| 出典データセット | uspto-grants-2002_09 |
| ORD ID | ord-e9d416b7d51d4e6ea08d5dbeef19cf5f |
| 出典メモ | uspto-grants-2002_09 |