反応式
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[C:6](=[O:17])(OC(Cl)(Cl)Cl)OC(Cl)(Cl)[Cl:9]>>[C:6]([C:2]1[NH:1][CH:5]=[CH:4][N:3]=1)([C:2]1[NH:1][CH:5]=[CH:4][N:3]=1)=[O:17].[ClH:9].[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1参加物
4
実験手順
Reaction of imidazole with bis (trichloromethyl) carbonate produces carbonyl diimidazole and crystalline imidazole hydrochloride. Insoluble imidazole hydrochloride is removed from the reaction mixture quantitatively by filtration and the carbonyl diimidazole is recovered by removing the solvent or crystallization under cooling or a combination thereof.
出典と根拠
- ORDレコード
- ord-f734730a142b45d28a7983dd411b3709
- 出典データセット
- uspto-grants-2002_09
- 特許番号
- US06455702B1
関連ノート
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