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Hexyl isocyanate → 1-Butyl-3-hexyl-1-(4-methyl-2-oxazolyl)urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexyl isocyanate | HCID 75659 | — |
| 反応物 | 2-Oxazolamine, N-butyl-4-methyl- | HCID 12295226 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 1-Butyl-3-hexyl-1-(4-methyl-2-oxazolyl)urea | HCID 23468965 | — |
反応手順
A solution of 2-butylamino-4-methyloxazole (10.0 g, 0.065 mol) and hexyl isocyanate (8.25 g, 0.065 mol) in dry benzene was heated under reflux for 3 hours. The solution was evaporated and the residual oil dissolved in ether, washed with dilute HCl, dried and re-evaporated. The residue was dissolved in petroleum spirit (40°-60° C.) carbon treated and re-evaporated under vacuum to give the pure product as a pale oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259343 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-202fc56c130343d9bcce6157dc42da0f |
| 出典メモ | uspto-grants-1981_03 |