Ethyl isothiocyanate → HCID 21519704、化合物
反応式
[C:1]([C:5]1[CH2:6][CH2:7][NH:8][CH2:9][CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:11]([N:13]=[C:14]=[S:15])[CH3:12]>O1CCCC1>[CH2:11]([NH:13][C:14]([N:8]1[CH2:7][CH:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH2:10][CH2:9]1)=[S:15])[CH3:12]参加物
4
実験手順
In 20 ml. of anhydrous tetrahydrofuran there is dissolved 5.0 grams of 4-t-butyl-1,2,3,6-tetrahydropyridine. Stirring is initiated and there is added 3.14 grams of ethylisothiocyanate in 10 ml. of anhydrous tetrahydrofuran allowing the reaction to run at room temperature. After stirring the reaction mixture for 18 hours, the tetrahydrofuran is evaporated in vacuo to give N-ethyl-4-t-butyl-1,2,3,6-tetrahydro-1-pyridinethiocarboxamide.
後処理
- customto run at room temperature
- stirringAfter stirring the reaction mixture for 18 hours
- customthe tetrahydrofuran is evaporated in vacuo
出典と根拠
- ORDレコード
- ord-ad7a2e1bbe2747feab55afc80d6d5c0b
- 出典データセット
- uspto-grants-1976_08
- 特許番号
- US03974283
反応ノート
読み込み中…