Hydrochloric Acid → molybdenum N,N-dimethylaniline

HRID 128362

反応式

HRID 128362 の反応式
Cl.[CH3:2][N:3]([CH3:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[NH4+].[O-][Mo:13]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O>O>[Mo:13].[CH3:2][N:3]([CH3:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

参加物

5

反応物 3

HCID 313Hydrochloric Acid2 回HCID 949N,N-DimethylanilineHCID 21895884Azanium bis(dioxido(dioxo)molybdenum)

生成物 1

HCID 131710929molybdenum N,N-dimethylaniline

試薬・触媒・溶媒 1

HCID 962Water溶媒3 回

実験手順

N,N-dimethylaniline molybdate having a 2/1 molybdenum/N,N-dimethylaniline molar ratio was prepared in the presence of HCl as follows. 10 grams of N,N-dimethylaniline, 16.26 grams of a 37 wt.% aqueous HCl solution, and 250 ml water were dissolved together and heated to reflux in a 500 ml round-bottomed flask equipped with a water-cooled condenser. 28.05 grams of ammonium dimolybdate was dissolved in 52 ml hot water and then added to the first solution.

後処理

  1. temperatureheated
  2. temperatureto reflux in a 500 ml round-bottomed flask
  3. temperaturecooled condenser
  4. additionadded to the first solution

出典と根拠

ORDレコード
ord-fee8ae2b43064c838c7c11ff8310f491
出典データセット
uspto-grants-1981_03
特許番号
US04259491

関連ノート

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