Thionyl Chloride → 4-(2-Cyanoethyl)benzoyl chloride
反応式
[C:1]([CH2:3][CH2:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][CH:6]=1)#[N:2].S(Cl)([Cl:16])=O>>[C:1]([CH2:3][CH2:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([Cl:16])=[O:10])=[CH:7][CH:6]=1)#[N:2]参加物
3
実験手順
A mixture of 17.5 parts of 4-(2-cyanoethyl) benzoic acid and 120 parts of thionyl chloride are refluxed for 15 minutes. The surplus thionyl chloride is then eliminated under reduced pressure and the 4-(2-cyanoethyl) benzoyl chloride is obtained which is liquid at atmospheric temperature.
後処理
- temperatureare refluxed for 15 minutes
出典と根拠
- ORDレコード
- ord-95030aba77e9410f92b623f38cd26edd
- 出典データセット
- uspto-grants-1976_10
- 特許番号
- US03987027
反応ノート
読み込み中…