Isopropylamine → HCID 21482733、化合物

HRID 1288316ノート

反応式

HRID 1288316 の反応式
[Br:1][C:2]1[CH:3]=[C:4]([S:9](Cl)(=[O:11])=[O:10])[CH:5]=[C:6]([Br:8])[CH:7]=1.[CH:13]([NH2:16])([CH3:15])[CH3:14]>O>[Br:1][C:2]1[CH:3]=[C:4]([S:9]([NH:16][CH:13]([CH3:15])[CH3:14])(=[O:11])=[O:10])[CH:5]=[C:6]([Br:8])[CH:7]=1

参加物

4

反応物 2

HCID 6363IsopropylamineHCID 214827463,5-Dibromobenzene-1-sulfonyl chloride

生成物 1

HCID 21482733HCID 21482733、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

3.0 G. of 3,5-dibromobenzenesulfonylchloride is added to a solution of 17.7 g. of isopropylamine in 25 ml. of water at room temperature. A complete solution results which is stirred for two hours and poured onto 250 ml. of water. The precipitate is filtered, washed with water, and dried affording 3,5-dibromo-N-isopropylbenzenesulfonamide, m.p. 105° to 107° C.

後処理

  1. customat room temperature
  2. customA complete solution results which
  3. additionpoured onto 250 ml
  4. filtrationThe precipitate is filtered
  5. washwashed with water
  6. customdried

出典と根拠

ORDレコード
ord-c705980d6b07435585286d52117154f9
出典データセット
uspto-grants-1976_10
特許番号
US03987199

反応ノート

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