Benzene → Phenylthionophosphonic dichloride

HRID 1288486

反応式

HRID 1288486 の反応式
[P:1]([Cl:5])(Cl)([Cl:3])=[S:2].[CH:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([P:1]([Cl:5])([Cl:3])=[S:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

参加物

3

反応物 2

HCID 241BenzeneHCID 19883Thiophosphoryl chloride

生成物 1

HCID 19016Phenylthionophosphonic dichloride

反応条件

温度
200 °C

実験手順

In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.

後処理

  1. temperaturethe mixture was heated
  2. additionThe reaction mixture was treated in accordance with the process of Example 1

出典と根拠

ORDレコード
ord-3415756249a948d698066d8c2ad191f4
出典データセット
uspto-grants-1976_10
特許番号
US03988368

関連ノート

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