Benzene → Phenylthionophosphonic dichloride
反応式
[P:1]([Cl:5])(Cl)([Cl:3])=[S:2].[CH:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([P:1]([Cl:5])([Cl:3])=[S:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1参加物
3
反応条件
- 温度
- 200 °C
実験手順
In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.
後処理
- temperaturethe mixture was heated
- additionThe reaction mixture was treated in accordance with the process of Example 1
出典と根拠
- ORDレコード
- ord-3415756249a948d698066d8c2ad191f4
- 出典データセット
- uspto-grants-1976_10
- 特許番号
- US03988368
反応ノート
読み込み中…