Thionyl Chloride → 2-(Chloromethyl)-6-methylnaphthalene
反応式
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]=[C:7]([CH2:12]O)[CH:6]=[CH:5]2.S(Cl)([Cl:16])=O>C1C=CC=CC=1>[Cl:16][CH2:12][C:7]1[CH:6]=[CH:5][C:4]2[C:9](=[CH:10][CH:11]=[C:2]([CH3:1])[CH:3]=2)[CH:8]=1参加物
4
実験手順
20.3 g. of 6-methyl-2-naphthalenemethanol is dissolved in 100 ml. of dry benzene and to this solution is added 30 ml. of thionyl chloride. The solution is stirred for about one hour and concentrated to yield 2-chloromethyl 6-methylnaphthalene.
後処理
- concentrationconcentrated
出典と根拠
- ORDレコード
- ord-be97f8851ab442e2a31052c5e03f4ac4
- 出典データセット
- uspto-grants-1976_10
- 特許番号
- US03988457
反応ノート
読み込み中…