Sodium → HCID 14518763、化合物

反応式

[P:1]([C:5]1([P:15]([OH:18])([OH:17])=[O:16])[CH:13]=[C:12]2[C:7]([CH:8]=[CH:9][CH2:10][NH+:11]2[CH3:14])=[CH:6]1)([OH:4])([OH:3])=[O:2].[Na]>>[CH3:14][N:11]1[CH:12]2[CH:7]([CH2:6][C:5]([P:15]([OH:17])(=[O:16])[OH:18])([P:1]([OH:3])(=[O:2])[OH:4])[CH2:13]2)[CH2:8][CH2:9][CH2:10]1

参加物

反応物 2

HCID 5360545Sodium

HCID 86752568Dihydro-6,6-diphosphono-1-methyl-1-pyrindinium

生成物 1

HCID 14518763HCID 14518763、化合物

実験手順

Dihydro-6,6-diphosphono-1-methyl-1-pyrindinium inner salt, monosodium salt [prepared as described in Example 4 hereinbefore] is hydrogenated using essentially the same procedure as described in Example 1 (part B) hereinbefore to provide octahydro-1-methyl-1-pyrindine-6,6-diphosphonic acid.

出典と根拠

ORDレコード: ord-a59784259c16427aabca76a53f4d9072
出典データセット: uspto-grants-1998_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05753634

反応ノート

読み込み中…