Methyl iodide → 131988-12-0

HRID 1291436ノート

反応式

HRID 1291436 の反応式
[CH3:1][I:2].[CH2:3]([O:5][C:6]1[C:10]([C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][C:6]1[C:10]([C:11]2[CH:12]=[N+:13]([CH3:1])[CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 15180131Pyridine, 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)- (9CI)

生成物 1

HCID 15819042131988-12-0

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(3-ethoxy-1,2,5-thiadiazol-4-yl) pyridine (520 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.72 g (83%).

後処理

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.72 g (83%)

出典と根拠

ORDレコード
ord-db1908e9f7ab4d9283c9c3fbdce12260
出典データセット
uspto-grants-1998_05
特許番号
US05753683

反応ノート

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