4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene
反応式
[CH:1]1[C:6]([OH:7])=[CH:5][CH:4]=[C:3]([Br:8])[CH:2]=1.[CH:9]([O:11][CH3:12])=[CH2:10]>>[Br:8][C:3]1[CH:4]=[CH:5][C:6]([O:7][CH:9]([O:11][CH3:12])[CH3:10])=[CH:1][CH:2]=1参加物
3
実験手順
Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.
後処理
- customas described in Synthesis Example 1, (1),
- distillationthe crude oil (24 g) was purified by distillation under reduced pressure
出典と根拠
- ORDレコード
- ord-24808c6fb6474ee0bab5996c316c4c25
- 出典データセット
- uspto-grants-1995_11
- 特許番号
- US05468589
反応ノート
読み込み中…