Ethylamine → 2-Chloro-N-ethyl-5-hydroxybenzamide

HRID 1295405

反応式

HRID 1295405 の反応式
[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH2:12]([NH2:14])[CH3:13]>>[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][C:3]=1[C:4]([NH:14][CH2:12][CH3:13])=[O:6]

参加物

3

反応物 2

HCID 6341EthylamineHCID 4582102-Chloro-5-hydroxybenzoic acid

生成物 1

HCID 589074862-Chloro-N-ethyl-5-hydroxybenzamide

実験手順

The title compound was prepared from 2-chloro-5-hydroxybenzoic acid and ethylamine, using a method similar to that used for preparation 52, as a colourless solid. 1HNMR (400 MHz, CDCl3) δ: 1.22 (3H, t), 3.42–3.49 (2H, m), 6.48–6.52 (1H, m), 6.80 (1H, dd), 7.13 (1H, d), 7.38 (1H, d); LRMS ESI m/z 200 [M+H]+

後処理

  1. customthat used for preparation 52, as a colourless solid

出典と根拠

ORDレコード
ord-1887cb4f412d407db3003ab77cc1f53a
出典データセット
uspto-grants-2007_07
特許番号
US07241810B2

関連ノート

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