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N-(Phenylacetyl)-L-alanine → 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| 反応物 | 4-Aminoazepan-2-one | HCID 21584138 | — |
| 生成物 | 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam | HCID 10215097 | — |
反応手順
Following General Procedure B above using N-(phenylacetyl)-L-alanine (Example A) and 3-aminocaprolactam (Sigma), the title compound was prepared as a solid having a melting point of 200-202° C. The reaction was monitored by tlc on silica gel (Rf=0.30 in 1:9 methanol/dichloromethane).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07390801B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-987c3041d8ff4f4fa979fdca053d055a |
| 出典メモ | uspto-grants-2008_06 |