Methyl Ethyl Ketone → Ethanol heptane

HRID 13563

反応式

HRID 13563 の反応式
Cl.N([C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)C=NN=1)N.[CH3:14][C:15](=[O:18])CC>CO.O>[CH2:15]([OH:18])[CH3:14].[CH3:4][CH2:13][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

参加物

4

反応物 2

HCID 6569Methyl Ethyl KetoneHCID 9351Hydralazine Hydrochloride

生成物 1

HCID 22502148Ethanol heptane収率 78%

試薬・触媒・溶媒 1

HCID 22242641Methanol--water (1/1)溶媒

実験手順

A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].

後処理

  1. customAfter evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone

出典と根拠

ORDレコード
ord-38722a7553584aeca29efcd3a8985b6f
出典データセット
uspto-grants-2010_06
特許番号
US07728133B2

関連ノート

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