Methyl Ethyl Ketone → Ethanol heptane
反応式
Cl.N([C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)C=NN=1)N.[CH3:14][C:15](=[O:18])CC>CO.O>[CH2:15]([OH:18])[CH3:14].[CH3:4][CH2:13][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]参加物
4
実験手順
A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].
後処理
- customAfter evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone
出典と根拠
- ORDレコード
- ord-38722a7553584aeca29efcd3a8985b6f
- 出典データセット
- uspto-grants-2010_06
- 特許番号
- US07728133B2
反応ノート
読み込み中…