化工社化工社 化学情報印刷レポート · 研究参考用
Acetone → Phthalazin-1-ylhydrazine;propan-2-ylidenehydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | Hydralazine Hydrochloride | HCID 9351 | — |
| 生成物 | Phthalazin-1-ylhydrazine;propan-2-ylidenehydrazine | HCID 86590016 | — |
反応手順
1-hydrazinophthalazine HCL (395 mg; 2 mmoles) is dissolved in 2.5 ml of acetone and allowed to react for 1 hour. The solvent is evaporated and the slightly yellow material is dried in vacuo to yield 411 mg of 1-hydrazinophthalazine acetone hydrazone. (99% of theoretical yield). [British Journal of Pharmacology 61: 345-349 (1977)]
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728133B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-fa33aa04990b413da75cdd22ca1aab4e |
| 出典メモ | uspto-grants-2010_06 |