Thionyl Chloride → 2-(Chloromethyl)-1,3-dimethoxybenzene

HRID 1357029

反応式

HRID 1357029 の反応式
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5]O.S(Cl)([Cl:15])=O>C1C=CC=CC=1>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5][Cl:15]

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 2776839(2,6-Dimethoxyphenyl)methanol

生成物 1

HCID 127070022-(Chloromethyl)-1,3-dimethoxybenzene

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

0.43 g (2.56 mmol) of 2,6-dimethoxybenzyl alcohol was dissolved in 5 ml of benzene, and the resultant solution was added with 0.40 g (3.36 mmol) of thionyl chloride at a room temperature. The mixture was then stirred for an hour at a room temperature to facilitate the provided compounds to react. The reacted solution was then condensed under reduced pressure to obtain a crude product of 2,6-dimethoxybenzyl chloride.

後処理

  1. customto react
  2. customcondensed under reduced pressure

出典と根拠

ORDレコード
ord-76f7ae5875dc448b82673af386701706
出典データセット
uspto-grants-2003_07
特許番号
US06589967B1

関連ノート

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