Thionyl Chloride → 2-(chloromethyl)-1,3-dimethoxyBenzene

HRID 1357031

反応式

HRID 1357031 の反応式
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5]O.S(Cl)([Cl:15])=O>C1C=CC=CC=1>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5][Cl:15]

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 2776839(2,6-Dimethoxyphenyl)methanol

生成物 1

HCID 127070022-(chloromethyl)-1,3-dimethoxyBenzene

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

0.49 g (2.93 mmol) of 2,6-dimethoxybenzyl alcohol was dissolved in 6 ml of benzene, and the resultant solution was added with 0.41 g (3.32 mmol) of thionyl chloride at a room temperature. The thus obtained solution was then stirred for 1.5 hours at a room temperature to complete a reaction. The reacted solution was then condensed under reduced pressure to obtain a crude product of 2,6-dimethoxybenzyl chloride.

後処理

  1. customa reaction
  2. customcondensed under reduced pressure

出典と根拠

ORDレコード
ord-18eef18fd527480fadf8042441fb3020
出典データセット
uspto-grants-2003_07
特許番号
US06589967B1

関連ノート

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