4-Fluorobenzylic alcohol → 4-Fluorobenzoic Acid
反応式
Br([O-])(=O)=[O:2].[Na+].[F:6][C:7]1[CH:14]=[CH:13][C:10]([CH2:11][OH:12])=[CH:9][CH:8]=1>C(#N)C.O>[F:6][C:7]1[CH:14]=[CH:13][C:10]([C:11]([OH:2])=[O:12])=[CH:9][CH:8]=1参加物
4
実験手順
The separated catalyst was added to a fresh batch of sodium bromate (0.3 g) and 4-fluorobenzyl alcohol (0.256 g, 2 mmol) in acetonitrile:water (1:1, 10 ml). The above procedure was repeated to give 4-fluorobenzoic acid as a white solid (0.25 g, 88%).
出典と根拠
- ORDレコード
- ord-3613e9979b044dd4a9ed5815f48c5a94
- 出典データセット
- uspto-grants-2010_06
- 特許番号
- US07728159B2
反応ノート
読み込み中…