Toluene → HCID 21079864、化合物
反応式
C1(C)C=CC=CC=1.ClC1C(=O)C(C#N)=C(C#N)C(=O)C=1Cl.[F:22][S:23]([CH:28]1[C:37]2[C:32](=[CH:33][CH:34]=[CH:35][CH:36]=2)[CH2:31][CH:30]=[CH:29]1)([F:27])([F:26])([F:25])[F:24]>CCCCC>[F:22][S:23]([C:28]1[C:37]2[C:32](=[CH:33][CH:34]=[CH:35][CH:36]=2)[CH:31]=[CH:30][CH:29]=1)([F:27])([F:26])([F:25])[F:24]参加物
5
反応条件
- 温度
- 65 °C
実験手順
Toluene and dichlorodicyanobenzoquinone (2 equivalents) were added to the product of step 2 and heated to 65° C. The reaction was monitored by GC. When the reaction was complete pentane was added. Resulting solids were removed by filtration. Color was removed by filtering through silica. The crude product was isolated by removing the solvent using rotary evaporation.
後処理
- additionwas added
- customResulting solids
- customwere removed by filtration
- customColor was removed
- filtrationby filtering through silica
出典と根拠
- ORDレコード
- ord-8ce6d48b03bc43dfb989b909d22d32cf
- 出典データセット
- uspto-grants-2007_01
- 特許番号
- US07166755B2
反応ノート
読み込み中…