反応式
CC([O:5][C:6](=[O:40])[CH2:7][CH2:8][CH2:9][NH:10][C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19][S:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[C:27]([NH:29][CH2:30][CH2:31][CH2:32][C:33]([O:35]C(C)(C)C)=[O:34])=[O:28])=[O:12])(C)C.FC(F)(F)C(O)=O.C1(OC)C=CC=CC=1>ClCCl>[C:22]1([C:27]([NH:29][CH2:30][CH2:31][CH2:32][C:33]([OH:35])=[O:34])=[O:28])[CH:23]=[CH:24][CH:25]=[CH:26][C:21]=1[S:20][S:19][C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=1[C:11]([NH:10][CH2:9][CH2:8][CH2:7][C:6]([OH:40])=[O:5])=[O:12]参加物
5
実験手順
This compound was prepared according to the procedure described in Example 50 using 4,4'-[dithiobis(2,1-phenylenecarbonylimino)]bis butanoic acid bis (1,1-dimethylethyl) ester (0.5 g, 0.9 mmol) from Example 43, 10 mL dichloromethane, 10 mL trifluoroacetic acid, and 1 mL anisole. The crude product was recrystallized from methanol/dimethylformamide/water to afford 0.6 g of the title compound, mp 165°-166° C.
後処理
- customThis compound was prepared
- customThe crude product was recrystallized from methanol/dimethylformamide/water
出典と根拠
- ORDレコード
- ord-03ab817d720446708337ba226b13df4e
- 出典データセット
- uspto-grants-1997_09
- 特許番号
- US05668291
関連ノート
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