Allyl chloride → HCID 22608987、化合物
反応式
[Na].[C:2]([NH:5][C:6]#[N:7])(=[O:4])[CH3:3].[CH2:8](Cl)[CH:9]=[CH2:10]>S1(CCCC1)(=O)=O>[C:6]([N:5]([CH2:10][CH:9]=[CH2:8])[C:2](=[O:4])[CH3:3])#[N:7]参加物
5
実験手順
159.1 g (1.5 mols) of the sodium salt of acetylcyanamide and 137.8 g (1.5 mols+20% excess) of allyl chloride are reacted in 400 ml of sulfolane for 9 hours and 45 minutes at 70°-127° C. analogously to Example 1, and the mixture is worked up in accordance with Example 1. This gives 121.7 g (65.4% of theory) of a colourless distillate, boiling at 98° C./43 mbar.
出典と根拠
- ORDレコード
- ord-07c999ba208745f099eef1a0ee27c832
- 出典データセット
- uspto-grants-1986_04
- 特許番号
- US04579933
反応ノート
読み込み中…