2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide

HRID 1380473

反応式

HRID 1380473 の反応式
[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([N:9]=[C:10]=[O:11])[N:3]=1.[CH:12]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[S:20]([NH2:23])(=[O:22])=[O:21])=[CH2:13]>C(#N)C>[Cl:8][C:6]1[N:7]=[C:2]([Cl:1])[N:3]=[C:4]([NH:9][C:10]([NH:23][S:20]([C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[CH:12]=[CH2:13])(=[O:21])=[O:22])=[O:11])[N:5]=1

参加物

4

反応物 2

HCID 113674032-EthenylbenzenesulfonamideHCID 130526242,4-Dichloro-6-isocyanato-1,3,5-triazine

生成物 1

HCID 20218271N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.

後処理

  1. customThe mixture is then evaporated under reduced pressure

出典と根拠

ORDレコード
ord-1656e35c0a6340cfb2e723df0ac630a5
出典データセット
uspto-grants-1986_04
特許番号
US04582525

関連ノート

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