Methanol → Methyl 2-(2-(aminomethyl)phenyl)acetate hydrochloride
反応式
Cl.[NH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH2:10][C:11]([OH:13])=[O:12].S(Cl)([Cl:16])=O.[CH3:18]O>>[ClH:16].[NH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH2:10][C:11]([O:13][CH3:18])=[O:12]参加物
4
実験手順
2-(Aminomethyl)-benzeneacetate hydrochloride was stirred in dry methanol. Thionyl chloride (1.1 eq.) was added dropwise and the mixture was stirred at room temperature overnight to provide for (methyl 2-(aminomethyl)-benzeneacetate hydrochloride as a white solid.
出典と根拠
- ORDレコード
- ord-e17361771d3a4d9ea8c7301b5968ecfc
- 出典データセット
- uspto-grants-2001_07
- 特許番号
- US06262302B1
反応ノート
読み込み中…