2-Methyl-3-[4-(2-methylbutan-2-yl)phenyl]prop-2-en-1-ol → 2-Methyl-3-(4-(tert-pentyl)phenyl)propan-1-ol
反応式
[C:1]([C:6]1[CH:11]=[CH:10][C:9]([CH:12]=[C:13]([CH3:16])[CH2:14][OH:15])=[CH:8][CH:7]=1)([CH2:4][CH3:5])([CH3:3])[CH3:2].[H][H]>[Pd]>[C:1]([C:6]1[CH:7]=[CH:8][C:9]([CH2:12][CH:13]([CH3:16])[CH2:14][OH:15])=[CH:10][CH:11]=1)([CH2:4][CH3:5])([CH3:2])[CH3:3]参加物
4
実験手順
70 g of 3-(p-tert.amyl-phenyl)-2-methyl-allyl alcohol are dissolved in 700 ml of alcohol, treated with 7 g of 5% palladium/carbon and hydrogenated until the hydrogen uptake has been completed. The catalyst is subsequently filtered and the alcohol is evaporated. By distillation there is obtained pure 3-(p-tert.amyl-phenyl)-2-methyl-propanol of boiling point 124°-129° C./0.04 Torr.
後処理
- filtrationThe catalyst is subsequently filtered
- customthe alcohol is evaporated
- distillationBy distillation there
出典と根拠
- ORDレコード
- ord-a4457355c5234f16b2b7ac5c68dd416d
- 出典データセット
- uspto-grants-1980_05
- 特許番号
- US04202894
反応ノート
読み込み中…