Buspirone Hydrochloride → Buspirone

HRID 1402639

反応式

HRID 1402639 の反応式
[CH:1]1[CH:2]=[N:3][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:25][CH2:24][CH2:23][CH2:22]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:5][CH:6]=1.Cl>CCO>[CH:1]1[CH:6]=[N:5][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:22][CH2:23][CH2:24][CH2:25]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:3][CH:2]=1

参加物

3

反応物 1

HCID 36431Buspirone Hydrochloride

生成物 1

HCID 2477Buspirone

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

0.2 grams of Phospholipin 90 were dissolved in 2.5 grams EtOH; to this solution 0.02 grams of Vitamin E were added and mixed to obtain a clear system. To this system, 0.2 grams of buspirone HCl dissolved in 7.08 grams DDW were slowly added under constant stirring at room temperature in Heidolph mixer (700 rpm). The obtained system was stirred for additional 5 minutes.

後処理

  1. additionmixed
  2. customto obtain a clear system
  3. additionwere slowly added
  4. stirringThe obtained system was stirred for additional 5 minutes

出典と根拠

ORDレコード
ord-bf8638285ae54532a2da69bf1f4e4edb
出典データセット
uspto-grants-2014_12
特許番号
US08911751B2

関連ノート

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