Thionyl Chloride → 3-Iodo-2-methoxy-benzoyl chloride
反応式
[I:1][C:2]1[C:3]([O:11][CH3:12])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](O)=[O:6].S(Cl)([Cl:15])=O>>[I:1][C:2]1[C:3]([O:11][CH3:12])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([Cl:15])=[O:6]参加物
3
反応条件
- 温度
- 82 °C
実験手順
To 3-iodo-2-methoxy-benzoic acid (8.29 g, 29.8 mmol) was added thionyl chloride (15 mL). The resulting solution was stirred for 2 minutes then heated to 82° C. and stirred at this temperature for 30 minutes. The solution was then concentrated under reduced pressure to give the title compound. This material was used without further purification.
後処理
- stirringstirred at this temperature for 30 minutes
- concentrationThe solution was then concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-a0dfb4ece7c749ea94dcf912cc5a2e6c
- 出典データセット
- uspto-grants-2014_12
- 特許番号
- US08912169B2
反応ノート
読み込み中…