Pinacol → Pinacol hexahydrate

HRID 1415076ノート

反応式

HRID 1415076 の反応式
[OH:1][C:2]([C:5]([OH:8])([CH3:7])[CH3:6])([CH3:4])[CH3:3].C(OOC(=O)C1C=CC=CC=1)(=[O:16])C1C=CC=CC=1>O>[OH2:1].[OH2:16].[OH2:1].[OH2:1].[OH2:1].[OH2:1].[OH:1][C:2]([C:5]([OH:8])([CH3:7])[CH3:6])([CH3:4])[CH3:3]

参加物

4

反応物 2

HCID 6425Pinacol2 回HCID 7187Benzoyl Peroxide

生成物 1

HCID 20268938Pinacol hexahydrate

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

In forming the structure of this example, the vinyl ester resin (available from The Dow Chemical Company under the tradename Derakane 411-45), the anhydrous pinacol and the water were preheated to about 52° C. The anhydrous pinacol and benzoyl peroxide were then dissolved in the vinyl ester resin with vigorous agitation. The water was then rapidly added with vigorous agitation continuing for a period of about 20 minutes to form an emulsion of pinacol hexahydrate in the resin. Thereafter, the dimethyl toluidine was added while mixing to form the final composition which was then poured into a mold. The composition set up quickly in the mold to form a rigid structure with the pinacol hexahydrate dispersed therein.

後処理

  1. customIn forming the structure of this example
  2. customwere preheated to about 52° C

出典と根拠

ORDレコード
ord-2827fee69e3249f3a43d0a02f0f95607
出典データセット
uspto-grants-1977_01
特許番号
US04003426

反応ノート

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