Hydrochloric Acid → 5-(Diethylamino)-2-methylphenol--hydrogen chloride (1/1)

HRID 1415079ノート

反応式

HRID 1415079 の反応式
[CH2:1]([NH:3][C:4]1[CH:5]=[CH:6][C:7]([CH3:11])=[C:8]([OH:10])[CH:9]=1)[CH3:2].[CH2:12](Br)[CH3:13].[ClH:15]>C(O)C>[ClH:15].[CH2:1]([N:3]([CH2:12][CH3:13])[C:4]1[CH:5]=[CH:6][C:7]([CH3:11])=[C:8]([OH:10])[CH:9]=1)[CH3:2]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 6332Ethyl BromideHCID 158012485-(Ethylamino)-2-methylphenol

生成物 1

HCID 203760655-(Diethylamino)-2-methylphenol--hydrogen chloride (1/1)

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

5 gm of 5-(ethylamino)-2-methylphenol were dissolved in 50 ml of ethanol, then alkylated analogously to the procedure described in Example 4 with 5,2 gm ethyl bromide, and worked up. The hydrochloride had a melting point of 192° C.

出典と根拠

ORDレコード
ord-21ace5bc68634e85ac9c5d52388a8e78
出典データセット
uspto-grants-1977_01
特許番号
US04003699

反応ノート

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