Trimethylamine → HCID 70632541、化合物

HRID 1415444ノート

反応式

HRID 1415444 の反応式
Br[CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5].CN[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH3:18][N:19](C)C>CCCCCC>[CH2:11]([CH2:18][NH:19][CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5])[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

参加物

5

反応物 3

HCID 1146TrimethylamineHCID 7669N-MethylbenzylamineHCID 21481846HCID 21481846、化合物

生成物 1

HCID 70632541HCID 70632541、化合物

試薬・触媒・溶媒 1

HCID 8058Hexane溶媒

反応条件

温度
100 °C

実験手順

To 0.25 moles of bromomethylmethyldimethoxysilane is added 0.25 moles of methylbenzylamine, and the mixture is heated to 100° C. for 12 hours. At the end of that time, 300 ml of hexane is added and excess trimethylamine is added. This mixture is allowed to stir for 3 hours, filtered, and the hexane is removed under reduced pressure, leaving benzylmethylaminomethylmethyldimethoxysilane.

後処理

  1. filtrationfiltered
  2. customthe hexane is removed under reduced pressure

出典と根拠

ORDレコード
ord-521d2d6b9e16418fa22849a04c213d75
出典データセット
uspto-grants-1977_01
特許番号
US04005118

反応ノート

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