化工社化工社 化学情報印刷レポート · 研究参考用
N-Methyl-D-glucamine → N-Methyl-D-glucamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Methyl-D-glucamine | HCID 8567 | — |
| 反応物 | Amoxicillin Trihydrate | HCID 62883 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-Methyl-D-glucamine | HCID 8567 | — |
| 生成物 | Amoxicillin | HCID 33613 | — |
反応手順
3 G. of N-methyl-D-glucamine are added to a suspension of 6 g. of amoxicillin trihydrate in 80 ml. of water and stirred at 5° C. Insoluble material is fitered off under suction and the resulting filtrate is lyophilized. There is thus obtained the N-methyl-D-glucamine salt of amoxicillin. Melting point: about 160° C. (decomposition). [α]D25 = + 133° (c =1 in water).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04005214 |
| 出典データセット | uspto-grants-1977_01 |
| ORD ID | ord-4bb8520051cd446fad35e01eb9c612fa |
| 出典メモ | uspto-grants-1977_01 |