Trimethylsilyl cyanide → HCID 21862842、化合物

反応式

[CH3:1][O:2][C:3]1[CH:20]=[CH:19][C:6]([CH:7]=[N:8][C:9]2[CH:14]=[CH:13][C:12]([S:15](=[O:18])(=[O:17])[NH2:16])=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.C[Si]([C:25]#[N:26])(C)C>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH:7]([NH:8][C:9]2[CH:14]=[CH:13][C:12]([S:15](=[O:18])(=[O:17])[NH2:16])=[CH:11][CH:10]=2)[C:25]#[N:26])=[CH:19][CH:20]=1

参加物

反応物 2

HCID 82115Trimethylsilyl cyanide

HCID 625902N-(4-Methoxybenzylidene)-4-sulfamoylaniline

生成物 1

HCID 21862842HCID 21862842、化合物

実験手順

Following a procedure similar to that described in Example 1(ii), but using N-(4-methoxybenzylidene)-4-sulfamoylaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a pale yellow powder (yield 98%).

出典と根拠

ORDレコード: ord-510b8fa0a9614265b9c8c13df9c2013a
出典データセット: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05908858

反応ノート

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