Trimethylsilyl cyanide → HCID 21862743、化合物

反応式

[CH2:1]([O:3][C:4]1[CH:21]=[CH:20][C:7]([CH:8]=[N:9][C:10]2[CH:15]=[CH:14][C:13]([S:16](=[O:19])(=[O:18])[NH2:17])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH3:2].C[Si]([C:26]#[N:27])(C)C>>[CH2:1]([O:3][C:4]1[CH:21]=[CH:20][C:7]([CH:8]([NH:9][C:10]2[CH:15]=[CH:14][C:13]([S:16](=[O:19])(=[O:18])[NH2:17])=[CH:12][CH:11]=2)[C:26]#[N:27])=[CH:6][CH:5]=1)[CH3:2]

参加物

反応物 2

HCID 82115Trimethylsilyl cyanide

HCID 6908344-[(4-Ethoxybenzylidene)amino]benzenesulfonamide

生成物 1

HCID 21862743HCID 21862743、化合物

実験手順

Following a procedure similar to that described in Example 1(ii), but using N-(4-ethoxybenzylidene)-4-sulfamoylaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a slightly yellow powder (yield 88%).

出典と根拠

ORDレコード: ord-c52a00b7c75a4f529c60b8c0afb6b30e
出典データセット: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05908858

反応ノート

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