Acrylic Acid → Trichlorogermylpropionic acid

反応式

[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[Cl:1][Ge:2]([CH:6]([CH3:7])[C:5]([OH:9])=[O:8])([Cl:4])[Cl:3]

参加物

反応物 2

HCID 6581Acrylic Acid

HCID 70900CID 70900

生成物 1

HCID 13587901Trichlorogermylpropionic acid

実験手順

Trichlorogermane (Cl3GeH) was added to acrylic acid (CH2CHCOOH) to obtain trichlorogermylpropionic acid (Cl3GeCH2CH2COOH). It was hydrolyzed to synthesize an organogermanium compound (1). In the same manner were synthesized organogermanium compounds (2) to (51).

出典と根拠

ORDレコード: ord-827b4ac667704e19b037162cd4fbe701
出典データセット: uspto-grants-1999_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05877311

反応ノート

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