Iodoethane → HCID 44295455、化合物
反応式
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[NH:9][C:10](=[S:16])[NH:11][CH2:12][C:13](N)=[O:14].[CH2:17](I)[CH3:18]>>[Cl:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[C:3]=1[N:9]1[C:13](=[O:14])[CH2:12][N:11]=[C:10]1[S:16][CH2:17][CH3:18]参加物
3
実験手順
The title compound was prepared by the procedure described in Example 2 using 27.8 g of 2-[3-(2,6-dichlorophenyl)-thioureido]-acetamide and 31.2 g of ethyl iodide. 12.8 g of the title compound was obtained, m.p. 122°-124° C. Anal. Calcd. for. C11H10Cl2N2O S: C, 45.69; H, 3.49; N, 9.69. Found: C, 45.62; H, 3.33; N, 9.43. Mass spectrum (+FAB, [M+H]+) m/z 289/291/293. 1H-NMR (DMSO-d6 ; 400 MHz) δ7.72 (s, 1 H), 7.70 (s, 1 H), 7.58 (t, 1 H), 4.50 (s, 2 H), 3.10 (q, 2 H), and 1.27 ppm (t, 3 H).
後処理
- customThe title compound was prepared by the procedure
出典と根拠
- ORDレコード
- ord-f42b47f1139847be903af1642b254195
- 出典データセット
- uspto-grants-1999_03
- 特許番号
- US05877324
反応ノート
読み込み中…